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- maleoyl acetoacetate 马来酸单酰乙酰乙酸,顺丁烯二酸单酰乙酰乙酸
- Nefedipine was synthesized with m-Nitrobenzaldehyde, ethyl acetoacetate, animonium acetate. 摘要以间硝基苯甲醛，乙酰乙酸乙酯，氨化试剂为原料。
- A1_20_3 sol is prepared by using Al(O-sec-Bu)3 chelated with ethyl acetoacetate(EAcAc) as precursor. 本文以乙酰醋酸乙酯(EAcAc)螯合的异丁醇铝为前驱物制备出了A1_20_3溶胶。
- Nefedipine was synthesized with m-Nitrobenzaldehyde,ethyl acetoacetate,ammonium acetate. 以间硝基苯甲醛,乙酰乙酸乙酯,氨化试剂为原料。
- METHODS Bropirimine was synthesized by 3 steps reaction of acylation, cyclization and bromination with ethyl acetoacetate as staring material. 方法以乙酰乙酸乙酯为起始原料,经酰化、环合、溴化3步反应合成溴匹立明。
- A new type of apple ester-B is synthesized by condensation reaction of ethyl acetoacetate and 1,2- propanediol,Using Fe 3+ -UR as catatlyst. 以Fe3 ＋ － UR 为催化剂，催化乙酰乙酸乙酯和1 ，2 － 丙二醇缩合反应合成了新型香料苹果酯－ B。
- Fructone was synthesized from ethyl acetoacetate and glycol using activated carbon supported phosphotungstic acid as catalyst. 以活性炭负载磷钨酸为催化剂合成了苹果酯,确定了反应的最优条件。
- With 1,4-bezenoquinone and ethyl acetoacetate as the starting materials, it had been prepared in a novel six-step procedure in overall yield of 34.6%. 以1，4-苯醌和乙酰乙酸乙酯为起始原料，经新的六步反应过程，合成阿比朵尔，总收率为34.;6%25。
- The strongly acidic cation exchange resin catalyzed synthesis of fructone-B by the reaction of ethyl acetoacetate and 1,2-propanediol was studied. 采用强酸性阳离子交换树脂为催化剂,以乙酰乙酸乙酯、1,2-丙二醇为原料合成苹果酯-B。
- Objective To investigate the chemical constituents of the extracts of Ledum palustre L.Var.Angustum E.Busch from acetoacetate. 摘要目的对细叶杜香乙酸乙酷部位的化学成分进行研究。
- Fructone-A and Fructone-B was synthesized from ethyl acetoacetate and ethanediol or 1,2-propanediol using ammonium ceric sulfate as catalyst. 以硫酸高铈铵为催化剂,通过乙酰乙酸乙酯分别与乙二醇和1,2-丙二醇反应合成了苹果酯-A和苹果酯-B,研究了催化剂等有关因素对产品收率的影响。
- The resulted IR Spectrum makes it possible to determine the reaction mechanism of ethyl acetoacetate with tetra butyl titanate. 得到的红外光谱使其决定钛酸四丁酯与乙酰乙酸乙酯的反应历程。
- N,N-Dihydroxyethyl-acetoacetamide,the raw material of the borate ester bonding agent,was synthesized from methyl acetoacetate and diethanolamine. 二乙醇胺与乙酰乙酸甲酯反应合成了硼酸酯键合剂原料N,N-二羟乙基乙酰乙酰胺。
- Method Compounds were extracted by 90% ethanol-petroleum ether and acetoacetate,then purified by silica gel column chromatography. 方法采用硅胶柱层析进行分离纯化,根据理化性质和波谱学数据进行结构鉴定。
- Optically active ethyl(S)-3-hydroxybutyrate,a useful chiral synthon,was prepared by stereoselective reduction of ethyl acetoacetate of the bread yeast in organic solvent. 利用面包酵母在非水相中不对称还原乙酰乙酸乙酯,制备了光学活性的手性化合物S()-3-羟基丁酸乙酯。
- The fraistone of new type perfume was synthesized with ethyl acetoacetate and 1,2 - propanediol as raw materials by the novel catalyst of polymer compound (FeCI3 - AICI3 - UR). 以乙酸乙酸乙酯和1，2一丙二醇为原料，在新型高分子复合催化剂FeCI3－AICI3－UR的催化作用下合成了新型香料草莓酯。
- Keto-enol tautomerizing of ethyl acetoacetate was studied by UV.It was conformed that the content of enol ethyl acetoacetate decreased with the increasing polarity of solvents. 本文以紫外光谱为手段研究乙酰乙酸乙酯的酮-烯醇式互变异构现象;所得结果证实其烯醇式含量随溶剂极性的增加而减少。
- Cefixime open side chain acid was prepared by oximation,etherification,chlorination,ester decomposition using t-butyl acetoacetate as starting material. 以乙酰乙酸叔丁酯为原料,经过肟化、醚化、氯代酯解反应合成了头孢克肟开环侧链酸。
- Several of costly solvents and chemicals such as DMF,dichloromethane,methyl acetoacetate,pivalic acid etc. left in waste liquid during the cephradine manufacturing process. 头孢拉定生产中的废液组分为DMF、二氯甲烷、特戊酸、乙酰乙酸甲酯和高沸点固体杂质,其中DMF、特戊酸、乙酰乙酸甲酯的经济价值均极高。
- Edaravone, a free radical scavenger, was synthesized by condensation of ethyl acetoacetate withphenylhydrazine in presence of NaHSO3 in water at pH 6 for 2h in a yield of 83%. 用苯肼和乙酰乙酸乙酯在亚硫酸氢钠参与下于水中回流反应2h制得自由基清除剂依达拉奉,收率83%25。方法操作简单,成本低。
