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- solid state reaction synthesis 固相合成
- A solid state reaction method is employed to synthesis nanometer-sized NiO and the overall procedure was monitored by FTIR, XRD, and EDS. 通过固相反应法制备了纳米NiO。 用FTIR,XRD,EDS等手段分析了固相反应制备纳米NiO的可行性和反应历程。
- Some new methods, solid state reaction by mechanical milling and liquid sta... 介绍了固相反应法、液相反应原位喷雾干燥法等加工纳米结构喷涂粉材的新方法。
- A new nonlinear optical material Ba 2Be 2B 2O 7 (Abbr.TBO) was synthesized by high temperature solid state reaction. 利用高温固相反应合成了一种新型的非线性光学材料Ba2 Be2 B2 O7(简称TBO)。 利用顶部熔盐籽晶法生长出了可供初步性能测试的TBO晶体。
- Traditionally, the most common method for preparing PTO and PZT powders was solid state reaction. 传统制备PTO以及PZT粉末最普遍的方法是采用固态法。
- The solid state reaction of 3-nitrobenzaldehyde and 2-thiobarbituric acid was carried out. 研究了3-硝基苯甲醛与硫代巴比妥酸固相反应,选择了反应的最佳条件。
- Three novel malononitrile derivatives have been synthesized by the solid state reaction at room temperature. 固相反应合成了新型丙二腈类化合物。
- synthesis by solid state reaction 固相反应合成法
- Negative thermal expansion (NTE) ZrW2O8 powders were synthesized using co-precipitation, solid state reaction and Sol-Gel route. 采用共沉淀法、分步固相法和溶胶凝胶法制备负热膨胀性ZrW2O8粉体。
- DTA, XRD and SEM analysis are applied to explore the processing conditions of Solid State Reaction for Mg2Si_(1-x)Ge_x(x=0,0.2,0.4,l) . 应用DTA、XRD、SEM等测试手段探索了固相反应制备Mg_2Si_(1-x)Ge_x(x=0;0.;2;0
- Nanoselenium was synthesized by the low temperature solid state reaction of Se02 with KI using SDS or CMC or PVP as the template. 用碘化钾还原二氧化硒,分别以十二烷基硫酸钠(SDS)、羧甲基纤维素钠(CMC)与聚乙烯吡咯烷酮(PVP)为软模板,低热固相反应制备纳米硒,并对其进行了表征,得到了各种不规则形状的纳米硒。
- Solid state reaction, co-precipitation, sol-gel and microemulsion are the common methods to prepare nano rare earth perovskite-type oxides. 稀土钙钛矿超微粉体的常规制备方法主要有机械混合法、化学共沉淀法、溶胶-凝胶法以及微乳液法等等。
- This study used the industrial zirconium oxide and silica as the main material to prepare the iron zircon pigment by solid state reaction. 采用工业用二氧化锆和二氧化硅为主要原料,通过固相合成方法制备了锆铁红色料。
- This paper reports a new method of preparing nanometer WS2 lubricating crystal using equipment of mechanical-physical solid state reaction. 报道了用机械-物理固相反应装置制备纳米WS2润滑材料的新方法。
- The results show that compared with the normal solid state reactions, the synthesis temperature and mean particle sizes of the pure KBT powders by MSS method are decreased greatly. 结果表明,与传统固相法相比,熔盐法合成温度显著降低且颗粒平均粒径明显减小。
- Compositely doped oxide La_(0.5)Sr_(0.5)CoO_(2.91)(LSC) was synthesized using solid state reaction and citric acid-nitrate low temperature self-propagating combustion methods. 采用固相反应法和柠檬酸-硝酸盐溶胶-凝胶低温自蔓延燃烧法(简称柠檬酸法)合成了La0.;5Sr0
- Transition metal complexes of hexamethylene tetramine are synthesized by solid state reaction and their thermochromism is investigated by TG-DSC spectra. 摘要研究了六次甲基四胺的过渡金属配合物的固相合成及其热色性。
- Several polycrystalline bismuth titanate Bi4Ti3O12(BTO)ceramic samples with different degrees of grain orientation(I)were prepared using the solid state reaction. 用固相烧结工艺制备了不同取向率(I)的Bi4Ti3O12(BTO)多晶陶瓷样品。
- ZHUANG Jia,CHI Yan-hua,WANG xi,et al.Study on nanophase Co3O4 fabrication by solid state reaction at ambient temperature[J].Journal of Inorgnic Materials,2001,16(6):1203-1206. [6]庄稼;迟燕华;王曦;等.;室温固相反应制备纳米Co3O4粉体[J]
- Lithium manganese oxides with different amount of Li/Mn molar ratio were synthesized by solid state reaction of EMD and Li2CO3. The influence of Li/Mn molar ratio on the structure and electrochemical characteristics of spinel LiMn2O4 is analyzed. 以电解二氧化锰和碳酸锂为原料用高温固相法合成了尖晶石锰酸锂;在锂与锰的原子比从0.;95:2到1