Tribenuronmethyl was synthesized in a two-step process involving esterification and amination using 2-methoxycarbonyl-sulfamoylbenzoate and methyl chloroformate as starting material.

• 由邻甲氧羰基苯磺酰胺和氯甲酸甲酯为起始原料,经过酯化、胺解二步反应合成了农药苯磺隆,确定了各步反应的较佳工艺条件。