The synthetic method of antinomy glycolate from Sb 2O 3 and excess HOC 2H 4OH with benzene as water carrying agent was studied by orthogonal experiment design.

• 以过量的乙二醇与三氧化二锑进行脱水反应,用苯为带水剂将生成的水带出,反应产物通过定性分析证明为乙二醇锑。