The mixture consisted of 0.05 mol SnCl4? 5 H2O, 1 mol MCPA, 3 mol isoocatnol and 1 000 ml cyclohexane as solvent was refluxed and dehydrated for 3 hours to give 0.9 mol MCPA-isoctyl in yield of 90% or more.

 
  • 将0.;05 mol四氯化锡、1 mol 2甲4氯酸、3 mol异辛醇和1000 ml溶剂环己烷;在升温回流带水条件下反应3 h;得到0
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