Determine DE confirm optimization of acid hydrolysis.The acid hydrolysis conditions were give as follows: acid concentration 6%, solvent media 95% EtOH, temperature 3h.

 
  • 75%25和85%25乙醇介质中反应产物的DE值较相对应的95%25乙醇介质中低,通过正交实验确定了水解适宜的工艺条件,酸解的最佳工艺条件为盐酸6%25、乙醇浓度95%25、时间3h。
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