A polyazamacrocycle C9H22N4 and its complex were synthesized. The crystal structure of [Ni(C9H22N4)](ClO4)2 was determined by X-ray diffraction method.

• 合成了氮杂大环配体C_9H_(22)N_4及其镍的配合物[Ni(C_9H_(22)N_4)](ClO_4)_2。 用X-射线衍射方法测定了配合物的晶体结构。