A micellar electrokinetic capillary chromatographic method (MECC ), using sodium benzoate as internal standard, for the determination of naringin and hesperidin in Chinese materia medica of Citrus L. was established.

• 建立了一种测定芸香科柑橘属药材中柚皮苷及橙皮苷含量的新方法，即以苯甲酸钠为内标物，采用胶束电动毛细管电泳法，可将上述药材中柚皮苷、橙皮苷和内标物较好分离。